Chem-Eng.21 |
1 1. HISTORY OF ANALYTICAL CHEMISTRY
- Classical methods: early years (separation of analytes) by precipitation, extraction or distilation.
- Qualitative: recognized by color, boiling point, solubility, taste.
- Quantitative: gravimetric or titrimetric measurements.
- Instrumental methods: Newer, faster, more efficient.
- Physical properties of analytes: conductivity, electrode potential, light emission absorption, mass to charge ratio and others.
2. 2. CLASSIFICAION OF MODERN ANALYTICAL METHODS
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- Gravimetric Methods determine the mass of the analyte or some compound chemically related to it.
- Electroanalytical Methods involve the measurement of such electrical properties as voltage, current, resistance, and quantity of electrical charge.
- Spectroscopic Methods are based on the measurement of the interaction between electromagnetic radiation and analyte atoms or molecules, or the production of such radiation by analytes
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Miscellaneous Methods include the measurement of such quantities as mass-to-charge ratio, rate of radioactive decay, heat of reaction, rate of reaction, sample thermal conductivity, optical activity, and refractive index.1. Analytical Methodology
- Understanding and Defining the Problem
- Analyzing and Reporting Results
- History of sample and background of the problem
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Component of analytical chemistry |
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